Course code:
1302S		 Course name:
Analytical chemistry 2

Academic year:

2012/2013.

Attendance requirements:

There are no requirements.

ECTS:

10

Study level:

basic academic studies

Study program:

Environmental Chemistry: 2. year, winter semester, compulsory course

Teacher:

Rada M. Baošić, Ph.D.
full professor, Faculty of Chemistry, Studentski trg 12-16, Beograd

Assistants:

Petar M. Ristivojević, Ph.D.
assistant professor, Faculty of Chemistry, Studentski trg 12-16, Beograd

Nikola R. Stevanović, Ph.D.

Hours of instruction:

Weekly: two hours of lectures + one hour of exercises + six hours of labwork (2+1+6)

Goals:

Acquisition of basic knowledge of quantitative chemical analysis (gravimetry and volumetry); introduction to the procedures of sampling of representative samples; selecting and applying the most appropriate methods; and assessment approaches in the course of solving problems in the analysis of complex ie. real samples; achievement skills, accuracy and precision in work.

Outcome:

A student is qualified to choose the method for quantitative analysis of the corresponding sample and to make the determination with the required accuracy and precision.

Teaching methods:

Lectures, labwork (group and individual) and theoretical exercises.

Extracurricular activities:

Student writing group exercises, solves problems and elaborates the principles of analysis.

Coursebooks:

Main coursebooks:

  • J. Savić, M. Savić: Fundamentals of analytical chemistry, Sarajevo
  • S. Mandić, R. Baošić, J. Mutić: Practicum of Analytical chemistry 2

Supplementary coursebooks:

  • D. A. Skoog, D. M. West, F. J. Holler: Fundamentals of analytical chemistry, 1999.

Additional material:

—

  Course activities and grading method

Lectures:

2 points (2 hours a week)

Syllabus:

  • Introduction; Classification.
  • Gravimetry; Examples of determination.
  • Introduction in volumetry; Classification; Titration curves; Standard solutions; Techniques.
  • Acid-base methods; Titration curves; Examples of determinations.
  • Nonaqueous titrations.
  • Precipitation methods; Titration curves; Examples of determinations.
  • Complexometry; Titration curves; Techniques; Selectivity; Applications.
  • Redox methods; Classification; Titration curves; Formal potential; Examples of determinations.
  • Sampling and translation of complex samples in solution.
  • Analysis of real sample.
  • Errors in quantitative analysis; Validation of obtained results.

Exercises:

3 points (1 hour a week)

Syllabus:

Problem solving and computational tasks.

Labwork:

38 points (6 hours a week)

Syllabus:

  • Gravimetry; Individual analysis.
  • Group exercises in acid-base methods; individual analysis.
  • Group exercises in methods of precipitation; individual analysis.
  • Group exercises in complexometry; individual analysis.
  • Group exercises in redox methods; individual analysis.
  • Preparation appropriate standard solutions and analysis of the real samples (ores or alloys).

Written exam:

30 points

Remarks:

Passed the written part of the exam is valid for two consecutive exam terms.

If the student collects a minimum of 35 points through the exam prerequisites, (s)he may be released from written exam and the written part of this win with 20 points.

Oral exam:

27 points