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Course code:
302H1

Course name:
Analytical Chemistry 2

Academic year:

2018/2019.

Attendance requirements:

101A1 + 301H1 + 301L1

ECTS:

10

Study level:

basic academic studies

Study programme:

Chemistry: 2. year, winter semester, compulsory course

Teacher:

Rada M. Baošić, Ph.D.
associate professor, Faculty of Chemistry, Studentski trg 12-16, Beograd

Assistants:

Aleksandra M. Dramićanin
assistant, Faculty of Chemistry, Studentski trg 12-16, Beograd

Slađana Z. Đurđić
assistant, Faculty of Chemistry, Studentski trg 12-16, Beograd

Olivera S. Marković
graduate researcher, Institute of Chemistry, Technology and Metallurgy, Njegoševa 12, Beograd

Hours of instruction:

Weekly: three hours of lectures + two hours of exercises + five hours of labwork (3+2+5)

Goals:

Helping students acquire knowledge of the basic principles of gravimetry and volumetry.

Outcome:

Students are trained and able to select the most suitable method and carry out sample analysis with appropriate accuracy and precision.

Teaching methods:

Lectures, experimental exercises (group and individual) and theoretical exercises.

Extracurricular activities:

After the classes which are organized with the aim of revising the subject matter of the course, students are expected to do problems on their own, to finish group exercises and prepare for the progress tests.

Coursebooks:

Main coursebooks:

  • J. Savić, M. Savić: Fundamentals of analytical chemistry, Sarajevo
  • R. Baošić, °.Lolić, J. Mutić, N. Stevanovic: Classical methods of quantitative chemical analysis, Belgrade, 2018

Supplementary coursebooks:

  • D. A. Skoog, D. M. West, F. J. Holler: Fundamentals of analytical chemistry, 1999.

Additional material:

Course activities and grading method

Lectures:

3 points (3 hours a week)

Syllabus:

  • Classification of quantitative methods of analysis; Basic principles of gravimetry; Some examples of gravimetric determinations.
  • Introduction to volumetry; Neutralization methods and their application.
  • Precipitation methods and their application.
  • Complexometry and its application.
  • Redox methods and their application.
  • The process of translating complex samples into a solution; real sample analysis.
  • Processing and validating results.

Exercises:

10 points (2 hours a week)

Syllabus:

Theoretical exercises - students do calculation problems and solve problems from certain areas of classical analytical chemistry (gravimetric and volumetric analyses).

At the end of the semester, students do a final test (10 points).

Labwork:

27 points (5 hours a week)

Syllabus:

  • Gravimetry. Analyses.
  • Group exercises / acid-base methods. Analyses.
  • Group exercises / precipitation methods. Analyses.
  • Group exercises / complexometry. Analyses.
  • Group exercises / redox methods. Analyses.

Experimental part (the maximum number of points - 27): The analysis conducted correctly the first time carries 3 points, each subsequent analysis conducted correctly carries 2 points.

Colloquia:

10 points

Remarks:

Progress tests (the maximum number of points - 10): students take the progress tests, on the lab session terms, after each area -  five of them; the students qualify for a progress test only after they have finished group exercises, which has to be verified by the teacher; the progress test consists of a problem which students have to do and a theoretical part. The progress test carries a total of 2 points; at one class session, a student has the right to take a test two times.

Written exam:

20 points

Oral exam:

30 points

Thu Feb 7 12:17:58 2019

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